10 Amphetamine: Excellent Response and Peak Symmetry 5 Drug Screen (GC/MS) 10 Column: Equity-5, 30m x 0.25mm ID, 0.25pm Cat. No.: 28089-U 15 Min Oven: 45°C (2 min) to 110°C @ 25°C/min to 200°C @ 15°C/min to 280°C Inj.: 250°C Det.: 5973 MSD, 40-450 amu scan range, 325°C transfer line Flow: Helium, 40psi for 0.2 min then 0.7mL/min constant flow Injection: 0.3μL pulsed splitless @ 50mL/min (0.5 min) Liner: Splitless 2mm ID Sample: -15ng on-column of a 16-component drug standard 2 6 3 1.2,4,5,6-Tetrachloro- m-xylene (surr.) 6. Heptachlor 7. Aldrin 2α-BHC 8. Heptachlor epoxide 3 B-BHC 9. +-Chlordane 4.1-BHC 10. Endosulfan! 5.&-BHC 8 10 11. a-Chlordane 10 1. Amphetamine 2. Methamphetamine 3. Nicotine 4. Caffeine 5. Diphenhydramine 6. Lidocaine 7. Phenobarbital 8. Methadone 9. Amitripyline 10. Cocaine 11. Desipramine 12. Codeine 13. Morphine 14. Diazepam 15. Heroin 16. Fentenyl 13 Key Resolutions Achieved 15 16 GOO1691 12 4,4'-DDE 13. Dieldrin 14. Endrin 15. Endosulfan Il 16 4,4'-DDD 17. Endrin aldehyde 18. Endosulfan sulfate 19. 4,4'-DDT 20. Endrin ketone 21. Methoxychlor 22. Decachlorobiphenyl (sum.) 11 12 13 15 20 16 1819 17 14 20 Min US EPA Method 8081 Chlorinated Pesticides (GC) Column: Equity-5, 30m x 0.25mm ID, 0.25μm Cat. No.: 28089-U Oven: 100°C (2 min) to 160°C @ 15°C/min to 300°C @ S°C/min (10 min) Inj.: 225°C Det.: ECD, 310°C Flow: Helium, 30cm/sec @ 100°C Injection: 2.0pt, splitless (0.5 min) Liner: Splitless double taper, unpacked Sample: 50ppb of a 22 component chlorinated pesticide standard (Cat. No. 46845-U) 21 - 30 22 GOO1689 13
10 Amphetamine: Excellent Response and Peak Symmetry 5 Drug Screen (GC/MS) 10 Column: Equity-5, 30m x 0.25mm ID, 0.25pm Cat. No.: 28089-U 15 Min Oven: 45°C (2 min) to 110°C @ 25°C/min to 200°C @ 15°C/min to 280°C Inj.: 250°C Det.: 5973 MSD, 40-450 amu scan range, 325°C transfer line Flow: Helium, 40psi for 0.2 min then 0.7mL/min constant flow Injection: 0.3μL pulsed splitless @ 50mL/min (0.5 min) Liner: Splitless 2mm ID Sample: -15ng on-column of a 16-component drug standard 2 6 3 1.2,4,5,6-Tetrachloro- m-xylene (surr.) 6. Heptachlor 7. Aldrin 2α-BHC 8. Heptachlor epoxide 3 B-BHC 9. +-Chlordane 4.1-BHC 10. Endosulfan! 5.&-BHC 8 10 11. a-Chlordane 10 1. Amphetamine 2. Methamphetamine 3. Nicotine 4. Caffeine 5. Diphenhydramine 6. Lidocaine 7. Phenobarbital 8. Methadone 9. Amitripyline 10. Cocaine 11. Desipramine 12. Codeine 13. Morphine 14. Diazepam 15. Heroin 16. Fentenyl 13 Key Resolutions Achieved 15 16 GOO1691 12 4,4'-DDE 13. Dieldrin 14. Endrin 15. Endosulfan Il 16 4,4'-DDD 17. Endrin aldehyde 18. Endosulfan sulfate 19. 4,4'-DDT 20. Endrin ketone 21. Methoxychlor 22. Decachlorobiphenyl (sum.) 11 12 13 15 20 16 1819 17 14 20 Min US EPA Method 8081 Chlorinated Pesticides (GC) Column: Equity-5, 30m x 0.25mm ID, 0.25μm Cat. No.: 28089-U Oven: 100°C (2 min) to 160°C @ 15°C/min to 300°C @ S°C/min (10 min) Inj.: 225°C Det.: ECD, 310°C Flow: Helium, 30cm/sec @ 100°C Injection: 2.0pt, splitless (0.5 min) Liner: Splitless double taper, unpacked Sample: 50ppb of a 22 component chlorinated pesticide standard (Cat. No. 46845-U) 21 - 30 22 GOO1689 13
Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter9: Atomic Absorption And Atomic Fluorescence Spectrometry
Section: Chapter Questions
Problem 9.6QAP
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