Based on the solubility data which solvent(s) used in this experiment would be an effective grease remover? Why is it so effective? Test tube Solvent Solubility (S or I) Solvent (P or NP) 1 Deionized water (H2O) I P 2 Ethanol (CH3CH2OH) I P 3 Hexane (CH3CH2CH2CH2CH2CH3) S NP 4 Dichloromethane (CH2Cl2) S

Based on the solubility data which solvent(s) used in this experiment would be an effective grease remover? Why is it so effective? Test tube Solvent Solubility (S or I) Solvent (P or NP) 1 Deionized water (H2O) I P 2 Ethanol (CH3CH2OH) I P 3 Hexane (CH3CH2CH2CH2CH2CH3) S NP 4 Dichloromethane (CH2Cl2) S

EBK A SMALL SCALE APPROACH TO ORGANIC L

4th Edition

ISBN:9781305446021

Author:Lampman

Publisher:Lampman

Chapter88: Column Chromatography

Section: Chapter Questions

Problem 5P

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Table of chemicals and reagents with their physicochemical properties (name, molecular formula, molecular weight, pKa, melting point, boiling point, etc.) Write a short outline or a flow diagram of the procedure List and safety issues Read and understand the MSDS information for each chemical used in this practical Experimental procedure Please do not scratch the clear sides of the UV cuvettes as this will invalidate your results. Part 1: Preparation of a calibration curve A calibration curve should be constructed using at least five concentrations of the pure paracetamol standard supplied in the range 3-15 ug/mL as follows: Weigh about 150 mg of paracetamol accurately and transfer to a 200 mL volumetric flask. Add 50 mL of o.1 M NaOH and dilute to about 100 mL with deionised water (DI). Shake and make up to volume with DI water. Dilute 10 mL of the resulting solution to 100 mL (volumetric flask) with DI water (= stock solution). Prepare standard solutions containing 3, 6, 9, 12 and 15…
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What is the concentration of hydrochloric acid? Find the concentration using the information given below. Equipment used in the lab: 50 mL burette X M H2SO4 solution (aq) • Two 50 mL beakers 0.10 M NaOH (aq) Procedure: 25 mL volumetric pipette • Bromothymol blue indicator • Pipette pump • 250 mL Erlenmeyer flask Observations from the Titration Lab. Trial 1 Trial 2 Trial 3 Final burette reading 14.6 mL 27.85 mL 40 mL Initial burette reading 0 mL 14.5 mL 27.85 mL Volume of H2SO4 (aq) added 25 mL 14.6mL 13.35 mL 12.15 mL
Students measured the concentration of HCl in a solution by titrating with different indicators to find the end point. (Use the table to find critical F values.) Mean HCl concentration (M) (+ standard deviation) Indicator Number of measurements 1. Bromothymol blue 0.09565 + 0.00170 28 2. Methyl red 0.08681 ± 0.00098 18 3. Bromocresol green 0.08641 + 0.00106 29 Is the difference between Indicators 1 and 2 significant at the 95% confidence level? O Yes O No Fenlculated clegrees of freedom Ecalculated Is the difference between indicators 2 and 3 significant at the 95% confidence level? O Yes O No Fealculated Spooled tcalculated
From a 10-mL sample, a 1-mL aliquot was taken and diluted to 100mL. From this, a 5-mL aliquot was taken and diluted to 20mL.The final 20mL was found to have a concentration of 0.004M analyte X.What is the concentration of analyte X in the 10-mL sample?
How many grams of NaAsO, should be weighed out to prepare a stock solution of 100 mg/L in 500 mL deionized water. Use the stock solution to prepare 4 different standard solution that can be used to prepare an analytical calibration curve to measure the concentration of 750 sample in the concentration range of 10-35 mg/L. Draw a proposed calibration curve (based on the results you achieved).
The sample containing 4.2 % NaCl will be determined gravimetrically as AgCl. What weight (in milligrams) of the sample must be taken to obtain a precipitate that will weigh about 0.39 mg? FM: NaCl = 58.44 AgCl = 143.3 %3D Answer in two decimal places. Do not include units in the answer. Answer:
25 ml of pickled brine was taken from an apple pickled with vinegar and diluted to 500 ml, 25 ml of this was taken and acidity was determined with 0.2 N (Factor: 1.05) NaOH. In the main trials, 6.3 ml - 6.5 ml - 6.9 ml, respectively, 0.1 ml base was used in the analysis without using the sample.For example, how many ppm is its acidity?
▪ In a blood alcohol analysis by GC-FID, methanol elutes at 1 min, ethanol at 2 min, IPA at 3 min, and IS at 4 min. In the patient sample, the analyte elutes t 2 min and the IS at 8 min. What is the relative retention time and the analyte in the patient? ▪ A) methanol B) Ethanol ▪ C) IPA
Concentration of Acetic Acid in a Vinegar Solution. Average molarity of NaOH Volume HC₂H30₂ sample Final buret reading Initial buret reading Volume NaOH (Show all units and all calculations) Molarity of HC₂H30₂ (unrounded) Average molarity of HC₂H302 (unrounded) Deviations Average deviation Best estimate for molarity of HC₂H302 Average mass percent HC₂H302 46.4mL Oml Ran out of Base ↓ ↓ ↓ ↓ 10.014 HOA je beart giov isults weari?! ferottelucuny Cambia) 10 Kousad Question 1. A Rolaids tablet contains calcium carbonate that neutralizes stomach acid. If 44.55 mL of 0.448 M hydrochloric acid is required to neutralize one tablet, how many milligrams of calcium carbonate are in a Rolaids tablet? CaCO, (s) + 2HCl(aq) → CaCl₂ (aq) + H₂O (1) + CO₂ (g)
Standardization of 0.10 M HCl1. Take three (3) clean and properly labeled 250-mL Erlenmeyer flasks. Into the three flasks, weigh 0.1 g of the primary standard Na2CO3 to the nearest 0.1 mg. Record the weights of the primary standard.2. Add about 75.0 mL of boiled distilled water and swirl to dissolve the solids.3. Add 2 to 3 drops of phenolphthalein indicator. Record the initial burette reading and titrate with the prepared 0.10 M HCl solution until phenolphthalein endpoint.4. Record the final burette reading for each titration in your data sheetDetermination of Ksp and Molar Solubility1. Add Ca(OH)2 to 250.0 mL distilled water with stirring until equilibrium is achieved. 2. Filter the undissolved precipitate. Measure out 50.0 mL of the supernate into a 250-mL Erlenmeyer flask using a pipette.3. Add a few drops of phenolphthalein indicator and titrate with standardized HCl solution until endpoint is achieved.4. Record the volume the HCl solution used. Perform two more trials.…
Standardization of 0.10 M HCl1. Take three (3) clean and properly labeled 250-mL Erlenmeyer flasks. Into the three flasks, weigh 0.1 g of the primary standard Na2CO3 to the nearest 0.1 mg. Record the weights of the primary standard.2. Add about 75.0 mL of boiled distilled water and swirl to dissolve the solids.3. Add 2 to 3 drops of phenolphthalein indicator. Record the initial burette reading and titrate with the prepared 0.10 M HCl solution until phenolphthalein endpoint.4. Record the final burette reading for each titration in your data sheetDetermination of Ksp and Molar Solubility1. Add Ca(OH)2 to 250.0 mL distilled water with stirring until equilibrium is achieved. 2. Filter the undissolved precipitate. Measure out 50.0 mL of the supernate into a 250-mL Erlenmeyer flask using a pipette.3. Add a few drops of phenolphthalein indicator and titrate with standardized HCl solution until endpoint is achieved.4. Record the volume the HCl solution used. Perform two more trials.…

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Test tube	Solvent	Solubility (S or I)	Solvent (P or NP)
1	Deionized water (H₂O)	I	P
2	Ethanol (CH₃CH₂OH)	I	P
3	Hexane (CH₃CH₂CH₂CH₂CH₂CH₃)	S	NP
4	Dichloromethane (CH₂Cl₂)	S	NP