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(40) Which of the following structures corresponds to the attached 1H-NMR spectrum?
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- Predict the ¹H shifts of the protons on the labeled carbons of the following chemical structure: OH NH₂ 1 2 a. H(1)=6.44, H(2)=6.40 b. H(1)=6.64, H(2)=6.60 c. H(1)-5.46, H(2)=5.40Isoamyl acetate is the primary component of artificial banana flavor. Which signals will be in the positive phase, negative phase, or nonexistent in normal 13C NMR, DEPT-90, and DEPT-135 of isoamyl acetate?4. Below are the IR regions and NMR chemical shifts table for use with the spectroscopy problems: 'H NMR 12 R O=C 11 OH 10 9 ΟΞΟ R-C-H 1---- - 00 8 Nitrogen-15 Oxygen-16 Nitrogen-14 7 Phosphorus-31 Sodium-23 Carbon-13 ppm 6 H C=C-H OH 5 NH H-C-X H-C-O -OH X = F, Cl, Br (i.e. electronegative atom) 3 -NH Which of the following isotopes is NOT NMR active? 2 H-C-N H-C-S 1 -CH3 -CH₂- CEC-H H-C-C=O -CH H-C-C=C HC-0 0 4000 DID small range range of values broad peak =C-H 3250- 3300 N-H broad with spikes -3300 3500 -O-H broad-3300 -3400 -O-H -CIN CO N-H H H 2730- 2820 -C-H of =C H 3000- 2 peaks 3100 2850- 2960 H O -C-O-H broad-3000 3000 usually strong -CEN 2200 -CICH ⇓ 2200 2500 wavenumber, cm-¹ 2000 C HC N H 1600- 1660 980 1680 AU OR 1730 O 1710 3 1600 NR₂ 1650 1500 1000 -1.
- he number of signals expected to be observed for CD2Cl2 solvent in CNMR is (I for D is 1) a) 1 b) 2 c) 3 Q2: Which of the following isotopes do not have quadrupole momet b) 27AI (I = 5/2) d) 5 e) 7 a) "Li (I = 3/2) %3D c) 170 (I = 5/2) d) 19F (I= 1/2) 23: Which of the following isotopes is expected to be NMR inactive? 12C b) 170 c) 31p d) 1°F e) 29Si : Consider the compound Fe3(CO)12, calculate %C (Fe 55.85 g/mol, C 12.1 gme c) 29.7 % e) 34.2 d) 28.6 % 30.7 % b) 6.13 %Q: Determine the structure of the following unknowns using the table to fill in your answers. B C B Signal 8 Integration Multiplicity Comments A C S J D C₂H₁0O₂ E 3 C10H120 PPM Signal & Integration Multiplicity Comments A 3 DOM L13C(1h) what is bracket mean in this case? is that mean carbon nmr proton nmr in same time?
- Interpret 1HNMR peaks of ethyl acetate include structureFor C NMR calculate the chemical shift in ppm for signals 1-7Total number of stereoisomers possible for the following compounds is HINT: a. 4 How many possible stereoisomers? How do we know how many stereoisomers are possible for a given structure? There is actually a straightforward way to figure this out. All we need to do is count the number of chiral centers and stereogenic alkene groups, the use this following rule: number of stereoisomeric forms = 2" ... where n = the number of chiral centers plus the number of stereogenic alkene groups b. 2 Consider for example a molecule with two chiral centers and one stereogenic alkene. By the rule stated above, we know right away that there must be eight possible stereoisomers. terminal alkene OH stereogenic alkene C. 8 OH d. 3 OH chiral center HO OH 3 2 = 8 T nonstereogenic alkenes (cannot be labelled E or Z) ←
- 4. NMR: (8 pts) Look at the given molecules and answer the following questions H H Compound A Compound B Compound C OH H Compound D How many different chemical environments (number of peaks) would you expect to see in the 'H NMR for each molecule? A = B = C = D: = Predict how many sub peaks per multiplet would be seen in the signal for the indicated hydrogen due to spin-spin splitting? A = B = C = D = How many H of that particular type (integration) would you expect to see at the indicated hydrogen? A = B = C = D= =Qu X Studen M Inbox Wordle | E Intro A Home Forest + data co E Project | Meetin Title + OASIS & Shared + O is.edu/courses/848465/quizzes/234535/take Question 17 Br A B OH ملا تو E OH C 6 pts G H D H F How many different signals would you expect to see in the 1H NMR of the given compounds? (i.e. different chemical shifts)? Compound A = Compound B = Compound C = Compound D = Compound E = Compound F = Search 10:28 PM 3/15/2024 4.26d Part 1 ✓ Your answer is correct. X Expected number of signals (enter a numerical value): 9 Mk