In most distillations, the total volume of liquid obtained (distillate + residue) is not equal to the volume of the mixture introduced into the flask. What are the possible sources of loss in this procedure?
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In most distillations, the total volume of liquid obtained (distillate + residue) is not equal to the volume of the mixture introduced into the flask. What are the possible sources of loss in this procedure?
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- 1,4‐Dimethoxybenzene (0.642 g) was dissolved in 2.0 mL acetic acid in a 25 mL Erlenmeyer flask using heat from a hot plate. Once the solid dissolved, 1.0 mL tert‐ butanol was added, and the reaction mixture was cooled in an ice bath. Then 2.0 mL concentrated sulfuric acid was added in 2‐3 drop portions,stirring the mixture after each aliquot. After the addition, the flask was removed from the ice bath and allowed to sit at room temperature for 15 minutes. Then 1.0 mL water was added dropwise to dilute the acid and the reaction mixture was added to 40 mL cold water in a 100 mL beaker. The solid was vacuum filtered and washed with 5 mL cold water, giving 52 g filtrate. The product wasrecrystallized from 4.5 mL methanol, yielding 0.317 g purified 1,4‐di‐tert‐butyl‐2,5‐dimethoxy benzene (27.2% yield). What is the atom economy, e-factor, and effective mass yield?In most distillations, the total volume of liquid obtained (distillate + residue) is not equal to the volume that was introduced into the flask. What are the possible sources of loss in this procedure?The NaOH titrant in this experiment was prepared to be approximately 0.1 M and then was standardized to determine its exact concentration. What possible reasons could there be for not simply weighing the solid NaOH, dissolving to a known volume and calculating its molarity?
- 25.0 cm3 of sodium hydroxide solution is tritrated against 0.2 mol dm–3 hydrochloric acid until the indicator just changes colour. 27.5 cm3 of the acid are required to reach the end point.Phenolphthalein is used as an indicator in the above experiment. What will be its colour change at the end point? From pink to yellow From pink to colourless From yellow to colourless From yellow to pinkVolumetric Analysis The mass of KHC8H4O4 is measured to the nearest milligram; however, the volume of water in which it is dissolved is never of concern—water is even added to the wall of the Erlenmeyer flask during the titration. Explain why water added to the KHC8H4O4 has no effect on the data, whereas water added to the NaOH solution, may drastically affect the data.Introductlon In Part (a) of this experiment you will prepare a primary standard. Potassium hydrogen phthalate (KHP) is a monoprotic acid with the formula KHC,H.O. In this experiment KHP is used as the primary standard. A standard solution is one whose solute concentration is accurately known. If a solute can be obtained in a very pure, stable, weighable form, a primary standard solution of it can be prepared directly. You will then use the standardized sodium hydroxide solution to determine the acetic acid content of a dilute unknown solution. Procedure (0) Preparation of a Primory Standard Potassium hydrogen phthalate (KHP) is a primary standard. Weigh accurately by difference, approximately 0.8 g of KHP in a clean, dry weighing bottle and transfer it into a 250 ml conical flask. Add 75 ml of distilled water. Swirl gently. Cover the flask and leave to dissolve, swirling periodicaly. Cautlon: KHP is not highly soluble and care must be taken to ensure it is all dissolved before you…
- In an extraction procedure, it is advisable to: O put the aqueous layer down the drain put the organic layer in the aqueous waste throw away all layers as soon as you have extracted them save all layers until an experiment is completeIn a similar experiment, the mass of 3 PB tablets was measured to be 3.1823 g. The tablets were crushed, and 2.9801 g of the powder was transferred to a beaker and reacted with HCl. After filtration, the filtrate was transferred to a 50-mL volumetric flask and diluted with water. 10.00 mL of this stock solution was combined with 0.2 M Na3PO4. The resulting precipitate weighed 0.2425 g after drying. What is the mass of BSS per tablet in mg?Round your answer to 1 decimal place.What are the applications of re-crystallization in gravimetric analysis? answer at your own words and answer should be to the point, not any irrelevant words
- The concentration of ammonia in a cleaning product was determined by back titration.Firstly, 10.00 cm3 of the cleaning product was pipetted into a large conical flask,containing 250.00cm3 of 0.50 mol/l HCl to give Solution A.Following a period of reaction and shaking, 50.00cm3 of Solution A was removed anddiluted to 250 cm3 with water in a volumetric flask to give Solution B.20 cm3 samples of Solution B were titrated against 0.05 mol/l Na2CO3 solution, givingan average titre of 12.45 cm3. i) Write equations for the reactions that have taken place.ii) Determine the concentration of NH3 in the original cleaning product in mol/l,g/l, ppm, and % w/v.In following these steps . Complete the table and provide th given chemical reactions in the qualitative analaysis of Group 3 Cations. Procedure 1. Place 20 drops of each of the following aqueous solutions to separate centrifuge tubes: 0.1M Cr (NO3)3, 0.1M Al (NO3)3, 0.1M Co (NO3)2, 0.1M Zn (NO3)2, 0.1M Mn (OH)2, 0.1M Ni (NO3)2, 0.1 M Fe (NO3)3. Make each solution basic by adding few drops of 6M NH4OH. Confirm using a litmus paper. 2. Add 5 drops of freshly prepared 6M (NH4)2S to each centrifuge tube. Place the samples in thecentrifuge machine for 3 mins. After centrifuge record results. Decant the supernatant liquid of all the samples. 3. Add one drop of NH4OH in each centrifuge tubes. Add 20 drops of distilled water in eachcentrifuge tubes. Then add a few drops of 6M HCl in each solution. Place the samples in the water bath for 10 mins. After water bath, centrifuge the samples for 3 mins. 4. After centrifuge, add a few drops of 6M NH4Cl in each sample. Decant the supernatant liquid…Write the balanced dissociation equation for solid mercury(I) acetate in aqueous solution. If it does not dissociate, simply write only NR. Be sure to include the proper phases for all species within the reaction.