IR Spectrum (liquid film) 4000 BO % of base peak 3000 20 40 80 13C NMR Spectrum (100.0 MHz, CDCI, solution) 105 DEPT CH₂ CH₂ CH proton decoupled 200 ¹H NMR Spectrum (400 MHz, CDCI, solution) 2000 jm 1600 1200 v (cm¹) Mt 120 120 160 m/e 160 800 Mass Spectrum CgH12 280 200 240 120 solvent 80 Problem 59 UV Spectrum Amax 261 nm (log, 2.7) max 269 nm (log, 2.5) solvent: methanol 40 08 (ppm) TMS 165

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter17: Applications Of Infrared Spectrometry
Section: Chapter Questions
Problem 17.4QAP
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What is the IR and HNMRAndCNMR and mass
58
4000
100
IR Spectrum
(liquid film)
282&
% of base peak
3000
40
80
13C NMR Spectrum
(100.0 MHz, CDCI, solution)
DEPT CH₂ CH₂ CH
proton decoupled
200
¹H NMR Spectrum
(400 MHz, CDCI, solution)
10
9
8
2000
105
v (cm'¹)
Mt 120
120
m/e
160
1600
160
7
m
1200
200 240
120
6
800
Mass Spectrum
CgH12
280
5
solvent
11
80
4
Problem 59
UV Spectrum
Amax 261 nm (log₁0 2.7)
max 269 nm (log,0€ 2.5)
solvent: methanol
3
40
2
08 (ppm)
TMS
0
8 (ppm)
1
165
Transcribed Image Text:58 4000 100 IR Spectrum (liquid film) 282& % of base peak 3000 40 80 13C NMR Spectrum (100.0 MHz, CDCI, solution) DEPT CH₂ CH₂ CH proton decoupled 200 ¹H NMR Spectrum (400 MHz, CDCI, solution) 10 9 8 2000 105 v (cm'¹) Mt 120 120 m/e 160 1600 160 7 m 1200 200 240 120 6 800 Mass Spectrum CgH12 280 5 solvent 11 80 4 Problem 59 UV Spectrum Amax 261 nm (log₁0 2.7) max 269 nm (log,0€ 2.5) solvent: methanol 3 40 2 08 (ppm) TMS 0 8 (ppm) 1 165
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