LOD D 4000 3000 2000 1500 1000 500 HAVENUMBERI -l 3331 13 1704 86 1266 47 970 21 667 64 2932 4. 1467 42 1238 53 926 84 557 53 2855 2606 68 2666 62 1452 29 17 1174 86 890 39 482 61 1963 1140 66 863 OH 1346 41 1068 11 845 47 2588 74 1329 50 1034 52 835 74 2233 84 1298 1026 32 789 64 TRANSMITTANCEI%!
LOD D 4000 3000 2000 1500 1000 500 HAVENUMBERI -l 3331 13 1704 86 1266 47 970 21 667 64 2932 4. 1467 42 1238 53 926 84 557 53 2855 2606 68 2666 62 1452 29 17 1174 86 890 39 482 61 1963 1140 66 863 OH 1346 41 1068 11 845 47 2588 74 1329 50 1034 52 835 74 2233 84 1298 1026 32 789 64 TRANSMITTANCEI%!
Chapter13: Structure Determination: Nuclear Magnetic Resonance Spectroscopy
Section13.SE: Something Extra
Problem 31AP: When measured on a spectrometer operating at 200 MHz, chloroform (CHCl3) shows a single sharp...
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Question
Identify all of the peaks in the spectrum. State the Experimental wavelength, Literature wavelength, peak characteristic, and assignment.
DOWN BELOW IS AN EXAMPLE...
Experimental Wavelength (cm-1) |
Literature wavelength (cm-1) |
Peak characteristic |
assignment |
3001cm-1, 3043cm-1 |
3010cm-1 |
sp2 C-H stretching |
|
2924cm-1 |
2900 -2980cm-1 |
sp3 C-H stretching |
Alkyl C-H |
1614cm-1 |
1500 -1650cm-1 |
C=C stretch |
alkene |
1443cm-1 |
1350-1450cm-1 |
C-H bend |
C-H |
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