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- Pls solve this question correctly in 5 min i will give u like for sure What evidence supports or refutes that during an experiment, purified extract is pure caffeine?g) h) i) j) H₂C Ph OCH3 HO OCH₂Ph OSI(CH₂)3 Br PPha + 2 1) "Buli /THF / rt/1.5 h 2) OsO4/ NalO4 acetone /ether LOCH3 -Si(CH3)3 CH3 /nt/1 h CH₂Cl₂-78°C / 15 min PPn, /1₂ (1 eq) imidazoie / THE 0°C - rt1%9V lli. O 1 M A;Yv 1. IF found impurity the melting point - Increase - Not effect - Decrease 2. benzoic acid can be purified by sublimation at . . pressure - high - low - normal 3. . . separates liquids with closer boiling points. * - fractional distillation - Extraction - Simple distillation with increasing 4. melting points molecular weight."
- C B) C) D) E) (C6H5)3P NH₂ Zn(Hg) HCI ۵۰۰ NaOH heat DMSO 1. Excess CH31 2. Ag₂O, H₂O 3. heat -O 53% 35°F Cloudy 12(4) Below are depictions of a student's TLC plates in which fractions 1 - 10 from their column are spotted. Lane 1 2 3 4 5 67 8 9 10 (a) Which fractions contain pure fluorenone? Which contain pure ferrocene? (b) Which lanes, if any, represent mixed fractions? (c) Would the student incorporate lanes 6 and 7 into an Erlenmeyer flask of a combined fraction? Explain with 10 words or less.T TrineOniline | Trine U in CH---214-01-5P-202 x E Problem Set 8.pdf 0 Mail - Outwater, Peri: X C Solvent Free Reduct x A New teb A Adobe Scan Apr 26. O File | CUsers/paris/Downloads/Problem%20Set%208.pdf 1 O A Page view A* Read aloud V Draw E Highlight v O Erase of 1 O Add text 1. In the Diels-Alder reaction below, six isomeric products A-F are depicted. However, only one of these is the major product formed. CM: OMe OMe CN .CN .CN OMe "Ma Me Ma CN OMs OMe OMe Me Me Me GN 'CN ON D E a) In the boxes above, label the diene and dienophile. b) Identify the two isomers that are unreasonable based on the concerted mechanism of the Diels-Alder reaction. (Hint: look at the geometry of the dienophile) Isomers: and c) Label the four remaining isomers as either endo or exo products. Endo: and Exo: and d) Of the two endo products, which would you predict to be favored based on regio- chemistry electronics? Explain your choice using resonance structures for full credit. Major Product: 41"F 2:05 PM…
- A student was asked to identify the best recrystallization solvent for compound X. Below is the experimental data obtained. Which is the best solvent of choice? Observations: vs= very soluble; so=soluble; ss= slightly soluble; in = insoluble Test tube 1 2 3 Solvent A B C Hot water bath vs vs ss Room temperature so ss in Ice water bath so in in Group of answer choices None B C Aa. Calculate the base saturation using the following given miliequivalent weights obtained from a 25g soil sample (a. Ca++= 2.23 m.e.; b. Mg++=1.32 m.e.; c. Na+= 1.98 m.e.; d. K+= 1.87 m.e.; e. H+= 1.27 m.e.; f. Al+++= 0.11 m.e.; g. NH4+= 2.3 m.e.; h. NO3-= 1.5 m.e. b. Calculate the CEC (m.e./100g soil) using the following given miliequivalent weights obtained from a 25g soil sample (a. Ca++= 2.23 m.e; b. Mg++=1.32 m.e.; c. Na+= 1.98 m.e.; d. K+= 1.87 m.e.; e. H+= 1.27 m.e.; f. Al+++= 0.11 m.e.; g. NH4+= 2.3 m.e.; h. NO3-= 1.5 m.e.Why acetone has les retention time and toluene has more. discus about polarity of 3 samples and interaction with stationary phase
- calculate the following for each sample gas chromatograph. a) retention time for each peak (label peaks) b) area of each peak c) %composition Sample GC of starting material for distillation of solution that is 40% ethyl acetate and 60% propyl acetate.Why does the %T on the spectrophotmete keep going up and down? It won't give an exact measurement.Temperature Wavelength A 0.64 g sample containing KCI ( mw = 74.6 ) is dissolved in 50mL of water and titrated to the Ag2CrO4 end point, requiring 26.2 mL of 0.15 * ? M AGNO3 .The %w/w KCI in the sample is 4. %3D Non of these 58.6% 45.8% 25.2% Which of the following alcohols would be most soluble in * ?water Heptanol O Hexanol Ethanol O Pentanol If 20mL of a 0.40M Mg(OH)2 solution is used to titrate 25mL of HCI