Macroscale and Microscale Organic Experiments
Macroscale and Microscale Organic Experiments
7th Edition
ISBN: 9781305577190
Author: Kenneth L. Williamson, Katherine M. Masters
Publisher: Brooks Cole
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Chapter 3, Problem 4Q
Interpretation Introduction

Interpretation:

The observed and the true melting point due to the rapid heating of the melting point bath should be compared.

Concept introduction:

Temperature at which an element changes from the solid state to the liquid state is known as melting point or sometimes liquefaction point. At the melting point, both solid and liquid phase coexist in equilibrium. It depends on the pressure and is normally defined at the standard pressure (1atm).

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A student obtained a solid product in a laboratory synthesis. To verify the identity of the solid, she measured its melting point and found that the material melted over a 10°C range. After it had cooled, she measured the melting point of the same sample again and found that this time the solid had a sharp melting point at the temperature that is characteristic of the desired product. Why were the two melting points different? What was responsible for the change in the melting point?
3. Pure benzophenone melts at 48.1°C. Your sample of benzophenone began to freeze at 47.0°C. When you repeated this measurement, the sample again began to freeze at 47.0°C. Give at least two reasonable explanations for this observation.
3. A student is trying to identify an unknown solid based on its melting point. She noted that the compound began to melt at 172°C and finished melting at 177°C. Knowing it is possible for there to be impurities in the sample, is this compound more likely to be camphor or hydroquinone. Explain your reasoning. 4. A young chemist has synthesized what he believed to be acetaminophen. He measured the melting point of this newly formed compound to be 163-178°C. If the literature value for the melting point of acetaminophen = 169-170.5°C, would the young chemist be wise to consume this product for headache relief? Why or why not?
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