Mean volume AgNO, Median volume AgNO, Standard deviation in the mean titration volume Confidence limit for the titration volume Relative confidence limit for the titration volume (standardization) - Concentration of AgNO, from mean titration volume mL ml. mL mL ppt mol L

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
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Chapter2: Crystallization
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Table A: Standard NaCl used to make primary standard solution
Mass of weighing bottle + NaC1 (g)
21.8720
Mass of weighing bottle after transfer (g)
21.772
Mass of NaCl used in solution (g)
0.6948
Purity of NaCl (%)
100.03
Table A: unknow used to make primary standard solution
Mass of weighing bottle + unknow (g)
16.8777
Mass of weighing bottle after transfer (g)
16.20010
Mass of unknow used in solution (g)
0.6776
Purity of unknow (%)
Table C: Titration of 25.00 mL aliquots of NaCl with AGNO3
Trial 1
Trial 2
Trial 3
Final Burette Reading (mL)
28.29
24.79
25.11
Initial Burette Reading (mL)
4.99
1.49
1.69
Volume Added (mL)
23.30
23.30
23.42
Table C: Titration of 25.00 mL aliquots of unknow with AGNO3
Trial 1
Trial 2
Trial 3
Final Burette Reading (mL)
Initial Burette Reading (mL)
23.99
22.45
26.91
2.89
1.25
5.61
Volume Added (mL)
21.10
21.20
21.30
Transcribed Image Text:Table A: Standard NaCl used to make primary standard solution Mass of weighing bottle + NaC1 (g) 21.8720 Mass of weighing bottle after transfer (g) 21.772 Mass of NaCl used in solution (g) 0.6948 Purity of NaCl (%) 100.03 Table A: unknow used to make primary standard solution Mass of weighing bottle + unknow (g) 16.8777 Mass of weighing bottle after transfer (g) 16.20010 Mass of unknow used in solution (g) 0.6776 Purity of unknow (%) Table C: Titration of 25.00 mL aliquots of NaCl with AGNO3 Trial 1 Trial 2 Trial 3 Final Burette Reading (mL) 28.29 24.79 25.11 Initial Burette Reading (mL) 4.99 1.49 1.69 Volume Added (mL) 23.30 23.30 23.42 Table C: Titration of 25.00 mL aliquots of unknow with AGNO3 Trial 1 Trial 2 Trial 3 Final Burette Reading (mL) Initial Burette Reading (mL) 23.99 22.45 26.91 2.89 1.25 5.61 Volume Added (mL) 21.10 21.20 21.30
Standard Sodium Chloride
Weighed mass of NaCI
g in 250.0 mL
Purity of NaCI
Molar concentration of NaCl using weighed mass and purity =
mol L-
Titrations of standard NacI (25.00 mL aliquots) with the provided AGNO;
Volume of AGN0, required (mL)
Precise Titration #
1
2
Mean volume AgNO,
mL
Median volume AGNO,
mL
Standard deviation in the mean titration volume
mL
Confidence limit for the titration volume
mL
Relative confidence limit for the titration volume (standardization) =
ppt
Concentration of AGNO, from mean titration volume
mol L-
3.
Transcribed Image Text:Standard Sodium Chloride Weighed mass of NaCI g in 250.0 mL Purity of NaCI Molar concentration of NaCl using weighed mass and purity = mol L- Titrations of standard NacI (25.00 mL aliquots) with the provided AGNO; Volume of AGN0, required (mL) Precise Titration # 1 2 Mean volume AgNO, mL Median volume AGNO, mL Standard deviation in the mean titration volume mL Confidence limit for the titration volume mL Relative confidence limit for the titration volume (standardization) = ppt Concentration of AGNO, from mean titration volume mol L- 3.
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